HT BSE detector

Imaging and measurement of surfaces in-situ and at high temperatures

Electrode-based detectors are specially designed for in-situ High Temperature experiments where conventional detectors cannot be used. This is, because light and thermal electrons emitted by the hot sample easily saturate the electronics, and because the unavoidable contamination from the in-situ conditions limits the lifetime of delicate sensors.

In this new design of the point electronic HT BSE Detektors, BackScattered Electrons (BSE) are absorbed in robust electrodes (metal plates) placed at the detection plane, the resultant absorbed current is preamplifier in-situ, and then amplified and mixed further ex-situ. Secondary and thermal electrons are repelled away, as a bias voltage is applied to the electrodes through the detector galvanic isolation. Light, either emitted from the hot sample, or scattered from a laser heater, does not produce signal in such technology, the detector is inherently light-blind.

Electrodes can be coated in various materials to optimise absorption efficiency at particular energy ranges, e.g. Carbon coating for higher acceleration voltages, and can be easily disassembled, cleaned and recoated.

Of course, four quadrant electrodes are used to enable 3D surface analysis when combined with our calibrated SEM scan controller (DISS6) and Topographic reconstruction software.

Quadrant electrodes

• Four metal electrodes with carbon coating
• Each electrode with own in-situ preamplifier
• Adjustable bias voltage applied to all
• Size and geometry adapted to SEM model

Easy to clean

• Entire detector front end is easily removed
• Electrodes can be cleaned and recoated as needed
• Screws are used for easy on-site disassembly
• Various electrode coatings may be reapplied

High Temperature

• Electrodes are blind to light emitted by hot samples
• Thermal electrons are filtered using the detector bias
• Maximum temperature limited only by radiative heating
• Compatible with laser heating

Quantitative measurements

• Electronic gains, offsets and bias are factory calibrated
• Amplification is temperature stabilized
• Current collected into sensing electrodes is measured
  (when combined with calibrated Scan controller for SEM (DISS6) and COMPO calibration sample)

Surface analysis

• TOPO and COMPO mix is done in the detector hardware
• 4Q signals are designed for topographic reconstruction
• Surface height/topography is measured
  (when combined with Scan controller for SEM (DISS6) and TOPO calibration sample)

> learn more about the specifications

Quantitative BSE

• map density with high-spatial resolution, even at high temperatures
• characterise phase transformation across a wide temperature range
• observe nucleation and growth of nano-materials

BSE Topography

• Analyse 3D surfaces and complex surfaces
• Monitor in-situ reactions, including high-temperature
• Distinguish between shape and density transformations

• HT BSE Detektor for LIMA-Arm, sample facing electrodes

  

• HT BSE detector for LIMA Arm, pole piece facing in-situ preamps

  

• Easy to clean and disassemble

  

• LIMA Arm retraction mechanism

  
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• BSE topography showing Cu catalyst during hydrogen oxidation